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ASTM C1524-02a(2010)
Standard Test Method for Water-Extractable Chloride in Aggregate (Soxhlet Method) (Withdrawn 2019)
4 стр.
Заменен
Печатное изданиеЭлектронный (pdf)
84.24 $ (включая НДС 20%)
Разработчик:
Зарубежные/ASTM
ICS:
91.100.30 Concrete. Including admixtures / Бетон и изделия из бетона
Сборник (ASTM):
04.02 Concrete and Aggregates / Бетон и заполнители для бетона
Тематика:
Cement & Concrete
Описание
Причина отменыThis test method provided procedures for sampling and analysis of aggregate for water-extractable chloride using a Soxhlet extractor.

Formerly under the jurisdiction of Committee C09 on Concrete and Concrete Aggregates, this test method was withdrawn in January 2019 in accordance with section 10.6.3 of the Regulations Governing ASTM Technical Committees, which requires that standards shall be updated by the end of the eighth year since the last approval date.

Значение и использование

Water-extractable chloride, when present in sufficient amount, has a potential to initiate or accelerate corrosion of metals, such as steel, embedded in or contacting a cementitious system, such as mortar, grout, or concrete. This test method is applicable when aggregates contain a high background of naturally occurring chloride (see ACI 222.196 ). Test Method C1152/C1152M determines acid-soluble chloride and Test Method C1218/C1218M determines water-soluble chloride. Both Test Methods C1152/C1152M and C1218/C1218M pulverize the sample to a fine powder or fine granular material. The Soxhlet method is intended to use nonpulverized material. Results with some aggregates have shown that the Soxhlet procedure extracts an extremely low amount of chloride, with most of it remaining in the rock, and therefore, it is not available for corrosion.

The Soxhlet extraction apparatus consists of three sections: the boiling flask, which contains reagent water at the beginning of the test; the extractor, which contains the sample inside a thimble; and, the condenser. The extractor functions by boiling the water, which condenses and drips on to the sample. When the water attains a fixed height above the sample, the extractor siphons the water from the thimble back to the boiling flask. The process repeats itself until the test is terminated. (Refer to Fig. 1.)

Область применения

1.1 This test method provides procedures for sampling and analysis of aggregate for water-extractable chloride using a Soxhlet extractor.

Note 1—This test method is to be used when significantly high chloride content has been found in aggregates, concretes, or mortars.

1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Ключевые слова:
aggregate; chloride content; Aggregate; Chloride analysis--concrete/aggregate; Soxhlet extraction; Water extraction