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ASTM D5910-05(2019)
Standard Test Method for Determination of Free Formaldehyde in Emulsion Polymers by Liquid Chromatography
6 стр.
Действует
Электронный (pdf)Печатное издание
78.00 $ (включая НДС 20%)
Разработчик:
Зарубежные/ASTM
ICS:
71.040.50 Physicochemical. Including spectrophotometric and chromatographic analysis / Физико-химические методы анализа. Включая спектрофотометрический и хроматографический анализы
Сборник (ASTM):
06.03 Paint –– Pigments, Polymers, Resins, Naval Stores, Cellulosic Esters, and Ink Vehicles / Красители – Пигменты, Быстровысыхающие масла, Полимеры, Смолы, Канифольно-скипидарные продукты, Целлюлозный полимер, Связующее вещества для красок
Тематика:
Paints & Related Coatings
Описание
Значение и использование

4.1 With the need to calculate free formaldehyde levels in emulsion polymers, it is necessary to make the determination without upsetting any equilibria that might generate or deplete formaldehyde. This test method provides a means for determining ppm levels of free formaldehyde in emulsion polymers without upsetting existing equilibria.

Область применения

1.1 This test method is used for the determination of free formaldehyde (HCHO) in emulsion polymers without upsetting existing formaldehyde equilibria. The procedure has been evaluated using acrylic, acrylonitrile-butadiene, carboxylated styrene-butadiene and polyvinyl acetate emulsion polymers. This test method may also be applicable for emulsion polymers of other compositions. The established working range of this test method is from 0.05 to 15 ppm formaldehyde. Emulsion polymers must be diluted to meet the working range.

1.2 This test method minimizes changes in free formaldehyde concentration that can result from changes in the physical or chemical properties of an emulsion polymer.

1.3 There are no known limitations to this test method when used in the manner described. The emulsion polymer test specimen must be prepared with a diluent that has a pH similar to that of the emulsion. Use of an inappropriate pH may upset formaldehyde equilibria and result in incorrect formaldehyde levels.

1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

Ключевые слова:
emulsion polymers; free formaldehyde; liquid chromatography; post-column reaction;