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ASTM D7740-11(2016)
Standard Practice for Optimization, Calibration, and Validation of Atomic Absorption Spectrometry for Metal Analysis of Petroleum Products and Lubricants
9 стр.
Заменен
Печатное изданиеЭлектронный (pdf)
96.72 $ (включая НДС 20%)
Разработчик:
Зарубежные/ASTM
ICS:
75.160.20 Liquid. Including gasoline, diesel, kerosene, etc. / Жидкое топливо75.100 Lubricants,. Including mineral oils, fluids for metal working and for temporary protection against corrosion / Смазки, индустриальные масла и связанные с ними продукты. Включая минеральные масла, жидкости для обработки металлов и для временной защиты от коррозии75.040 Crude petroleum / Сырая нефть71.040.50 Physicochemical. Including spectrophotometric and chromatographic analysis / Физико-химические методы анализа. Включая спектрофотометрический и хроматографический анализы
Сборник (ASTM):
05.04 Petroleum Products, Liquid Fuels, and Lubricants (IV): D6973–D7755 / Нефтепродукты, жидкое топливо и смазочные материалы (IV): D6973–D7755
Тематика:
Petroleum
Описание
Значение и использование

5.1 Accurate elemental analysis of petroleum products and lubricants is necessary for the determination of chemical properties, which are used to establish compliance with commercial and regulatory specifications.

5.2 Atomic Absorption Spectrometry (AAS) is one of the most widely used analytical techniques in the oil industry for elemental analysis. There are at least twelve Standard Test Methods published by ASTM D02 Committee on Petroleum Products and Lubricants for such analysis. See Table 1.

5.3 The advantage of using an AAS analysis include good sensitivity for most metals, relative freedom from interferences, and ability to calibrate the instrument based on elemental standards irrespective of their elemental chemical forms. Thus, the technique has been a method of choice in most of the oil industry laboratories. In many laboratories, AAS has been superseded by a superior ICP-AES technique (see Practice D7260).

5.4 Some of the ASTM AAS Standard Test Methods have also been issued by other standard writing bodies as technically equivalent standards. See Table 2.

(A) Excerpted from ASTM MNL44, Guide to ASTM Test Methods for the Analysis of Petroleum Products and Lubricants, 2nd edition, Ed., Nadkarni, R. A. Kishore, ASTM International, West Conshohocken, PA, 2007.

Область применения

1.1 This practice covers information on the calibration and operational guidance for elemental measurements using atomic absorption spectrometry (AAS).

1.1.1 AAS Related Standards—Test Methods D1318, D3237, D3340, D3605, D3831, D4628, D5056, D5184, D5863, D6732; Practices D7260 and D7455; and Test Methods D7622 and D7623.

1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Ключевые слова:
atomic absorption spectrometry; elemental analysis; fuels analysis; lubricant analysis;