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ASTM E177-08
Standard Practice for Use of the Terms Precision and Bias in ASTM Test Methods
12 стр.
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Разработчик:
Зарубежные/ASTM
ICS:
19.020 Test conditions and procedures in general / Условия и методика испытаний в целом
Сборник (ASTM):
14.05 Statistical Methods; Hazard Potential of Chemicals; Thermal Measurements; Manufacture of Pharmaceutical and Biopharmaceutical Products / Статистические методы; Потенциальная опасность химических веществ; Измерения теплопроводности; Производство фармацевтических изделий
Тематика:
Quality Control
Описание
Значение и использование

Part A of the Blue Book, Form and Style for ASTM Standards, requires that all test methods include statements of precision and bias. This practice discusses these two concepts and provides guidance for their use in statements about test methods.

PrecisionA statement of precision allows potential users of a test method to assess in general terms the test method's usefulness with respect to variability in proposed applications. A statement of precision is not intended to exhibit values that can be exactly duplicated in every user's laboratory. Instead, the statement provides guidelines as to the magnitude of variability that can be expected between test results when the method is used in one, or in two or more, reasonably competent laboratories. For a discussion of precision, see Section 15.

BiasA statement of bias furnishes guidelines on the relationship between a set of typical test results produced by the test method under specific test conditions and a related set of accepted reference values (see Section 16).

An alternative term for bias is trueness, which has a positive connotation, in that greater bias is associated with less favorable trueness. Trueness is the systematic component of accuracy.

AccuracyThe term accuracy, used in earlier editions of Practice E 177, embraces both precision and bias (see Section 17 and Note 3).

A Table of Contents is shown below, listing the concepts in this standard.

TABLE OF CONTENTSSection
GENERAL CONCEPTS
Test Method 5
Measurement Terminology 6
SOURCES OF VARIABILITY
Experimental Realization of a Test Method 7
Operator 8
Apparatus 9
Environment 10
Sample 11
Time 12
STATISTICAL CONCEPTS
Accepted Reference Value 13
Statistical Control 14
Precision 15
Bias 16
Accuracy 17
Variation of Precision and Bias with Material 18
Variation of Precision and Bias with Sources of Variability 19
COMBINATIONS OF SOURCES OF VARIABILITY
Repeatability and Laboratory Bias 20
Other Within-a-Single Laboratory Precisions 21
Reproducibility and Bias of the Test Method 22
Range of Materials 23
METHODS OF EXPRESSING PRECISION AND BIAS
Indexes of Precision 24
Preferred Indexes of Precision for ASTM Test Methods 25
Preferred Statements of Bias for ASTM Test Methods 26
Elements of a Statement of Precision and Bias 27
STATEMENTS OF PRECISION AND BIAS
Examples of Statements of Precision and Bias 28
Область применения

1.1 The purpose of this practice is to present concepts necessary to the understanding of the terms precision and bias as used in quantitative test methods. This practice also describes methods of expressing precision and bias and, in a final section, gives examples of how statements on precision and bias may be written for ASTM test methods.

1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory requirements prior to use.

Ключевые слова:
accepted reference value; accuracy; bias; interlaboratory study; precision; precision conditions; repeatability; reproducibility; standard deviation; Accuracy assessment; ASTM voluntary consensus standards; Bias; Measurement processes/systems; Precision--construction materials test methods; Statistical methods