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This document provides design and operating guidelines for sampling, sample handling and sample analysis of high water content streams, up to 50 % water by volume. As a guide, this RP targets a relative accuracy of 5 % of reading up to a maximum of 50 % water content as a qualifier for the various methods described herein. For example, the corresponding absolute accuracy for a 10 % water content stream is +/- 0.5 % and for 20 % water content is +/- 1.0 %.