5.1 This test method provides information on the uniaxial tensile properties and tensile stress-strain response of a ceramic composite tube—tensile strength and strain, fracture strength and strain, proportional limit stress and strain, tensile elastic modulus, etc. The information may be used for material development, material comparison, quality assurance, characterization, and design data generation.

5.2 Continuous fiber-reinforced ceramic composites (CFCCs) are composed of continuous ceramic-fiber directional (1D, 2D, and 3D) reinforcements in a fine-grain-sized (<50 µm) ceramic matrix with controlled porosity. Often these composites have an engineered thin (0.1 to 10 µm) interface coating on the fibers to produce crack deflection and fiber pull-out. These ceramic composites offer high-temperature stability, inherent damage tolerance, and high degrees of wear and corrosion resistance. As such, these ceramic composites are particularly suited for aerospace and high-temperature structural applications (1, 2).3

5.3 CFCC components have a distinctive and synergistic combination of material properties, interface coatings, porosity control, composite architecture (1D, 2D, and 3D), and geometric shape that are generally inseparable. Prediction of the mechanical performance of CFCC tubes (particularly with braid and 3D weave architectures) cannot be made by applying measured properties from flat CFCC plates to the design of tubes. Direct uniaxial tensile strength tests of CFCC tubes are needed to provide reliable information on the mechanical behavior and strength of tube geometries.

5.4 CFCCs generally experience “graceful” fracture from a cumulative damage process, unlike monolithic advanced ceramics which fracture catastrophically from a single dominant flaw. The tensile behavior and strength of a CFCC are dependent on its inherent resistance to fracture, the presence of flaws, and any damage accumulation processes. These factors are affected by the composite material composition and variability in material and testing—components, reinforcement architecture and volume fraction, porosity content, matrix morphology, interface morphology, methods of material fabrication, test specimen preparation and conditioning, and surface condition.

5.5 The results of tensile tests of test specimens fabricated to standardized dimensions from a particular material or selected portions of a part, or both, may not totally represent the strength and deformation properties of the entire, full-size end product or its in-service behavior in different environments.

5.6 For quality control purposes, results derived from standardized tubular tensile test specimens may be considered indicative of the response of the material from which they were taken, given primary processing conditions and post-processing heat treatments.

1.1 This test method determines the axial tensile strength and stress-strain response of continuous fiber-reinforced advanced ceramic composite tubes at ambient temperature under monotonic loading. This test method is specific to tube geometries, because fiber architecture and specimen geometry factors are often distinctly different in composite tubes, as compared to flat plates.

1.2 In the test method a composite tube/cylinder with a defined gage section and a known wall thickness is fitted/bonded into a loading fixture. The test specimen/fixture assembly is mounted in the testing machine and monotonically loaded in uniaxial tension at ambient temperature while recording the tensile force and the strain in the gage section. The axial tensile strength and the fracture strength are determined from the maximum applied force and the fracture force. The strains, the proportional limit stress, and the tensile modulus of elasticity are determined from the stress-strain data.

1.3 This test method applies primarily to advanced ceramic matrix composite tubes with continuous fiber reinforcement: unidirectional (1D, filament wound and tape lay-up), bidirectional (2D, fabric/tape lay-up and weave), and tridirectional (3D, braid and weave). These types of ceramic matrix composites are composed of a wide range of ceramic fibers (oxide, graphite, carbide, nitride, and other compositions) in a wide range of crystalline and amorphous ceramic matrix compositions (oxide, carbide, nitride, carbon, graphite, and other compositions).

1.4 This test method does not directly address discontinuous fiber-reinforced, whisker-reinforced, or particulate-reinforced ceramics, although the test methods detailed here may be equally applicable to these composites.

1.5 The test method describes a range of test specimen tube geometries based on past tensile testing of ceramic composite tubes. These geometries are applicable to tubes with outer diameters of 10 to 150 mm and wall thicknesses of 1 to 25 mm, where the ratio of the outer diameter-to-wall thickness (d_O /t) is typically between 5 and 30.

1.5.1 This test method is specific to ambient temperature testing. Elevated temperature testing requires high-temperature furnaces and heating devices with temperature control and measurement systems and temperature-capable grips and loading fixtures, which are not addressed in this test method.

1.6 The test method addresses test equipment, gripping methods, testing modes, allowable bending stresses, interferences, tubular test specimen geometries, test specimen preparation, test procedures, data collection, calculation, reporting requirements, and precision/bias in the following sections.

Section

Scope

1

Referenced Documents

2

Terminology

3

Summary of Test Method

4

Significance and Use

5

Interferences

6

Apparatus

7

Hazards

8

Test Specimens

9

Test Procedure

10

Calculation of Results

11

Report

12

Precision and Bias

13

Keywords

14

Annexes

Interferences

Annex A1

Test Specimen Geometry

Annex A2

Grip Fixtures and Load Train Couplers

Annex A3

Allowable Bending and Load Train Alignment

Annex A4

Test Modes and Rates

Annex A5

1.7 Units—The values stated in SI units are to be regarded as standard.

1.8 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 8.

1.9 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.