4.1 The test method described is useful as a rapid, nondestructive technique for in-place measurements of wet density and water content of soil and soil-aggregate and the determination of dry density.

4.2 The test method is used for quality control and acceptance testing of compacted soil and soil-aggregate mixtures as used in construction and also for research and development. The nondestructive nature allows repetitive measurements at a single test location and statistical analysis of the results.

4.3 Density—The fundamental assumptions inherent in the methods are that Compton scattering is the dominant interaction and that the material is homogeneous.

4.4 Water Content—The fundamental assumptions inherent in the test method are that the hydrogen ions present in the soil or soil-aggregate are in the form of water as defined by the water content derived from Test Methods D2216, and that the material is homogeneous. (See 5.2)

Note 1: The quality of the result produced by this standard test method is dependent on the competence of the personnel performing it, and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing/sampling/inspection, and the like. Users of this standard are cautioned that compliance with Practice D3740 does not in itself ensure reliable results. Reliable results depend on many factors; Practice D3740 provides a means of evaluating some of those factors.

1.1 This test method describes the procedures for measuring in-place density and moisture of soil and soil-aggregate by use of nuclear equipment (hereafter referred to as “gauge”). The density of the material may be measured by direct transmission, backscatter, or backscatter/air-gap ratio methods. Measurements for water (moisture) content are taken at the surface in backscatter mode regardless of the mode being used for density.

1.1.1 For limitations see Section 5 on Interferences.

1.2 The total or wet density of soil and soil-aggregate is measured by the attenuation of gamma radiation where, in direct transmission, the source is placed at a known depth up to 300 mm (12 in.) and the detector(s) remains on the surface (some gauges may reverse this orientation); or in backscatter or backscatter/air-gap the source and detector(s) both remain on the surface.

1.2.1 The density of the test sample in mass per unit volume is calculated by comparing the detected rate of gamma radiation with previously established calibration data.

1.2.2 The dry density of the test sample is obtained by subtracting the water mass per unit volume from the test sample wet density (Section 11). Most gauges display this value directly.

1.3 The gauge is calibrated to read the water mass per unit volume of soil or soil-aggregate. When divided by the density of water and then multiplied by 100, the water mass per unit volume is equivalent to the volumetric water content. The water mass per unit volume is determined by the thermalizing or slowing of fast neutrons by hydrogen, a component of water. The neutron source and the thermal neutron detector are both located at the surface of the material being tested. The water content most prevalent in engineering and construction activities is known as the gravimetric water content, w, and is the ratio of the mass of the water in pore spaces to the total mass of solids, expressed as a percentage.

1.4 Two alternative procedures are provided.

1.4.1 Procedure A describes the direct transmission method in which the probe extends through the base of the gauge into a pre-formed hole to a desired depth. The direct transmission is the preferred method.

1.4.2 Procedure B involves the use of a dedicated backscatter gauge or the probe in the backscatter position. This places the gamma and neutron sources and the detectors in the same plane.

1.4.3 Mark the test area to allow the placement of the gauge over the test site and to align the probe to the hole.

1.5 Units—The values stated in SI units are to be regarded as standard. The values given in parentheses are provided for information only and are not considered standard.

1.6 All observed and calculated values shall conform to the guide for significant digits and rounding established in Practice D6026.

1.6.1 The procedures used to specify how data are collected, recorded, and calculated in this standard are regarded as the industry standard. In addition, they are representative of the significant digits that should generally be retained. The procedures used do not consider material variation, purpose for obtaining the data, special purpose studies, or any considerations for the user’s objectives; and it is common practice to increase or reduce significant digits of reported data to be commensurate with these considerations. It is beyond the scope of this standard to consider significant digits used in analysis methods for engineering design.

1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.