These test methods detail the standard procedures for the chemical analysis of soaps containing synthetic detergents. The analytical procedures include the determination of the following chemical properties and substances: moisture and other matter volatile at a specified temperature; free alkali or free acid; anhydrous, salt-free soda soap; alcohol-soluble matter; matter insoluble in water; total alkalinity of matter insoluble in alcohol (alkaline salts); sodium silicate; phosphates; phosphates by colorimetric method using molybdenum blue); unsaponified and unsaponifiable matter; free fatty matter; chlorides in alcohol-soluble matter; rosin by McNicoll method; synthetic detergent by difference; and neutral inorganic salts.
Область применения1.1 These test methods cover procedures for the chemical analysis of soaps containing synthetic detergents.
1.2 The analytical procedures appear in the following order:
SectionsMoisture and Other Matter Volatile at 105°C (Oven Method)5 and 6Free Alkali or Free Acid7 and 8Anhydrous, Salt-Free, Soda Soap9-12Alcohol-Soluble Matter13 and 14Matter Insoluble in Water15Total Alkalinity of Matter Insoluble in Alcohol (Alkaline Salts)16 and 17Sodium Silicate18-20Phosphates21-28Phosphate (Colorimetric Method Using Molybdenum Blue)29-34Unsaponified and Unsaponifiable Matter35-39Free Fatty Matter40Chlorides in Alcohol-Soluble Matter41-43Rosin (McNicoll Method)44-47Synthetic Detergent (by Difference)48Neutral, Inorganic Salts491.3 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.