This test method calibrates or demonstrates conformity of thermogravimetric apparatus at ambient conditions. Most thermogravimetry analysis experiments are carried out under temperature ramp conditions or at isothermal temperatures distant from ambient conditions. This test method does not address the temperature effects on mass calibration.

In most thermogravimetry experiments, the mass change is reported as weight percent in which the observed mass at any time during the course of the experiment is divided by the original mass of the test specimen. This method of reporting results assumes that the mass scale of the apparatus is linear with increasing mass. In such cases, it may be necessary only to confirm the performance of the instrument by comparison to a suitable reference.

When the actual mass of the test specimen is recorded, the use of a calibration factor to correct the calibration of the apparatus may be required, on rare occasions.

1.1 This test method covers the calibration or performance confirmation of the mass (or weight) scale of thermogravimetric analyzers and is applicable to commercial and custom-built apparatus.

1.2 Electronic instrumentation or automated data analysis and reduction systems or treatments equivalent to this test method may be used.

1.3 The values stated in SI units are to be regarded as the standard.

1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and to determine the applicability of regulatory limitations prior to use.