These test methods for the chemical analysis of metals and alloys are primarily intended to test such materials for compliance with compositional specifications. It is assumed that all who use these test methods will be trained analysts capable of performing common laboratory procedures skillfully and safely. It is expected that work will be performed in a properly equipped laboratory.
Note—Shaded areas are suitable for sampling.
FIG. 1 Type A and Type B Disks Область применения1.1 These test methods cover the chemical analysis of aluminum and aluminum-base alloys having compositions within the following limits:
Beryllium, ppm0.3 to 100Bismuth, %0.02 to 1.0Boron, %0.005 to 0.060Cadmium, %0.001 to 0.50Chromium, %0.01 to 1.0Copper, %0.01 to 20.0Gallium, %0.001 to 0.05Iron, %0.01 to 3.0Lead, %0.01 to 1.0Lithium, %0.001 to 4.0Magnesium, %0.002 to 12.0Manganese, %0.005 to 2.0Nickel, %0.01 to 4.0Silicon, %0.05 to 20.0Tin, %0.03 to 1.0Titanium, %0.002 to 0.30Vanadium, %0.002 to 0.16Zinc, %0.003 to 12.0Zirconium, %0.01 to 0.301.2 The analytical procedures appear in the following order:
SectionsBeryllium by Argon Plasma Optical Emission Spectroscopy283 to 292Beryllium by the Morin (Fluorometric) Test Method8-19Bismuth by the Thiourea (Photometric) Method1aBismuth and Lead by the Atomic Absorption Test Method188 to 198Boron by the Carmine (Photometric) Test Method30 to 38Cadmium by the Atomic Absorption Test Method167 to 177Chromium:Diphenylcarbazide (Photometric) Test Method39 to 47Persulfate Oxidation (Titrimetric) Test Method1bChromium by the Atomic Absorption Test Method199 to 209Copper and Lead by the Electrolytic (Gravimetric) Test Method1cCopper and Zinc by the Atomic Absorption Test Method210 to 220Copper by the Electrolytic (Gravimetric) Test Method303 to 311Copper by the Neocuproine (Photometric) Test Method1aGallium by the Ion Exchange-Atomic Absorption Test Method312 to 323Iron by the 1,10-Phenanthroline (Photometric) Method73 to 81Iron and Manganese by the Atomic Absorption Method221 to 231Lithium by the Atomic Absorption Test Method324 to 334Magnesium:Pyrophosphate (Gravimetric) Method1 bEthylenediamine Tetraacetate (Titrimetric) TestMethod88 to 93Magnesium by the Atomic Absorption Test Method232 to 242Manganese by the Periodate (Photometric) Test Method 293 to 302Nickel:Dimethylglyoxime (Photometric) Test Method1aDimethylglyoxime (Gravimetric) Test Method1bNickel by the Atomic Absorption Test Method243 to 253Silicon:Molybdisilicic Acid (Photometric) Test Method118 to 127Sodium Hydroxide-Perchloric Acid (Gravimetric) Method128 to 133Tin by the Iodate (Titrimetric) Test Method134 to 140Titanium by the Chromotropic Acid (Photometric) Test Method 141 to 150Titanium by the Diantipyrylmethane Photometric Test Method254 to 263Vanadium by an Extraction-Photometric Test Methodusing N-Benzoyl- N-Phenylhydroxylamine264 to 273Zinc:Ammonium Mercuric Thiocyanate or the ZincOxide (Gravimetric) Test Method1 bEthylenediamine Tetraacetate (Titrimetric) Test Method 1dIon Exchange-EDTA Titrimetric Test Method274 to 282Zirconium by the Arsenazo III (Photometric) Method178 to 1871.3 The values stated in SI units are to be regarded as the standard.
1.4 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific hazard statements are given throughout these test methods.