This test method covers the determination of non-volatile matter, that is, residue on evaporation, in solvent extract from aerospace components, using a rotary flash evaporator. The summary of the test method, the apparatus for testing, reagents and materials for testing, and procedure for testing are all presented in details.
Область применения1.1 This test method covers the determination of nonvolatile matter, that is, residue on evaporation, in solvent extract from aerospace components, using a rotary flash evaporator.
1.2 The procedure for extraction from components is described in practices such as Practice F303. Before subjecting the extract to the following method, it should be processed to remove the insoluble particulate in accordance with Practice F311 (Note 1). Particle count analysis of the removed particulate may then be performed in accordance with Test Method F312. If particulate is not removed from the extract prior to performing this method, this should be noted on the test report.
Note 1—Membrane filters with a maximum extractable content of 0.5 weight % should be used on samples to be processed by this test method. Conventional membranes contain 5 to 10 % extractables. For obtaining very low background levels, consideration should be given to using membranes without grid marks.1.3 The values stated in SI units are to be regarded as standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.